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Green Chemistry Series
Ball Milling Towards Green Synthesis: Applications, Projects, Challenges
Edited by
Brindaban Ranu;
Brindaban Ranu
University of Jadavpur, India
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Achim Stolle
Achim Stolle
University of Jena, Germany
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Hardback ISBN:
978-1-84973-945-0
PDF ISBN:
978-1-78262-198-0
EPUB ISBN:
978-1-78262-348-9
Series:
Green Chemistry Series
No. of Pages:
303
Published online:
26 Nov 2014
Published in print:
05 Dec 2014
Book Chapter
CHAPTER 5: Cross Dehydrogenative Coupling Reactions by Ball Milling
By
Jingbo Yu
;
Jingbo Yu
Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, College of Pharmaceutical Sciences, Zhejiang University of Technology
Hangzhou
310014
China
[email protected]
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Zhijiang Jiang
;
Zhijiang Jiang
Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, College of Pharmaceutical Sciences, Zhejiang University of Technology
Hangzhou
310014
China
[email protected]
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Weike Su
Weike Su
Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, College of Pharmaceutical Sciences, Zhejiang University of Technology
Hangzhou
310014
China
[email protected]
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Published:26 Nov 2014
-
Series: Green Chemistry Series
Page range:
96 - 113
Citation
J. Yu, Z. Jiang, and W. Su, in Ball Milling Towards Green Synthesis: Applications, Projects, Challenges, ed. B. Ranu and A. Stolle, The Royal Society of Chemistry, 2014, pp. 96-113.
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Remarkable progress has been made in solvent-free cross-dehydrogenative coupling (CDC) reactions under high-energy ball milling conditions. This chapter will show the CDC and asymmetry CDC reaction between tetrahydroisoquinolines and several kinds of pronucleophiles, including active methylene compounds (sp3), terminal alkynes (sp) and indoles (aryl-sp2). Further attention is paid to the influence of the milling parameters, especially the influence of milling frequency on yield and enantioselectivity.
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