Aqueous Microwave Assisted Chemistry: Synthesis and Catalysis
The demands for green and sustainable synthetic methods in the fields of healthcare and fine chemicals, combined with the pressure to produce these substances expeditiously and in an environmentally benign fashion, pose significant challenges to the synthetic chemical community. Green chemistry can avoid pollution by utilizing techniques that are environmentally friendly by design and one of the best green techniques is the use of microwave (MW) assisted aqueous synthetic protocols. Fusing MW technique with water (as a benign reaction medium) can offer an extraordinary synergistic effect with greater potential than these two individual components in isolation. Selective microwave heating can be exploited to develop a high yield protocol and the use of water expedites the MW-protocol with more energy efficiency. This book provides an overview of the various processes developed using aqueous microwave chemistry and is written for chemists, chemical engineers and researchers in the early stages who want to develop sustainable and green processes. Written by well known microwave experts, the book is a comprehensive examination of the field and is the first book that deals strictly with aqueous microwave chemistry and represents a significant effort towards green chemistry. It covers all the microwave-assisted aqueous reactions in depth, including heterocycle synthesis, metal catalysis, enzyme catalysis, polymer synthesis, nanomaterials synthesis and nano-catalysis. Each chapter contains representative experimental procedures, helping the reader quickly replicate some of the experiments to gain hands-on experience.
Aqueous Microwave Assisted Chemistry: Synthesis and Catalysis, The Royal Society of Chemistry, 2010.
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Fundamentals of Aqueous Microwave Chemistryp1-9ByVivek Polshettiwar;Vivek PolshettiwarSustainable Technology Division, National Risk Management Research Laboratory, U.S. Environmental Protection Agency26 W. Martin Luther King Dr.MS 443CincinnatiOhio 45268USASearch for other works by this author on:Rajender S. VarmaRajender S. VarmaSustainable Technology Division, National Risk Management Research Laboratory, U.S. Environmental Protection Agency26 W. Martin Luther King Dr.MS 443CincinnatiOhio 45268USASearch for other works by this author on:
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Chapter 2: Metal-catalyzed Reactions in Water under MW Irradiationp10-54ByVictorio Cadierno;Victorio CadiernoDepartamento de Química Orgánica e Inorgánica, Instituto Universitario de Química Organometálica “Enrique Moles” (Unidad Asociada al CSIC), Facultad de Química, Universidad de OviedoJulián Clavería 833006OviedoSpainSearch for other works by this author on:Pascale Crochet;Pascale CrochetDepartamento de Química Orgánica e Inorgánica, Instituto Universitario de Química Organometálica “Enrique Moles” (Unidad Asociada al CSIC), Facultad de Química, Universidad de OviedoJulián Clavería 833006OviedoSpainSearch for other works by this author on:Sergio E. García-GarridoSergio E. García-GarridoDepartamento de Química Orgánica e Inorgánica, Instituto Universitario de Química Organometálica “Enrique Moles” (Unidad Asociada al CSIC), Facultad de Química, Universidad de OviedoJulián Clavería 833006OviedoSpainSearch for other works by this author on:
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Chapter 3: Microwave-assisted Coupling Reactions in Aqueous Mediap55-90ByAziz Fihri;Aziz FihriTransformations Intégrées de la Matière Renouvelable ESCOM-UTC, 1-Allée du Jean-Marie Buckmaster60200CompiègneFranceSearch for other works by this author on:Christophe LenChristophe LenTransformations Intégrées de la Matière Renouvelable ESCOM-UTC, 1-Allée du Jean-Marie Buckmaster60200CompiègneFranceSearch for other works by this author on:
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Chapter 4: Microwave-assisted Synthesis of Bio-active Heterocycles in Aqueous Mediap91-122ByVivek Polshettiwar;Vivek PolshettiwarSustainable Technology DivisionNational Risk Management Research LaboratoryU. S. Environmental Protection Agency26 W. Martin Luther King Dr.MS 443CincinnatiOhio45268USASearch for other works by this author on:Rajender s. VarmaRajender s. VarmaSustainable Technology DivisionNational Risk Management Research LaboratoryU. S. Environmental Protection Agency26 W. Martin Luther King Dr.MS 443CincinnatiOhio45268USASearch for other works by this author on:
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Chapter 5: Microwave-assisted Enzymatic Reactions in Aqueous Mediap123-144ByHua ZhaoHua ZhaoChemistry Program, Savannah State UniversitySavannahGA 31404USASearch for other works by this author on:
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Chapter 6: Microwave-assisted Synthesis of Polymers in Aqueous Mediap145-175ByCatherine Marestin;Catherine MarestinLaboratoire des Matériaux Organiques à Propriétés Spécifiques (LMOPS)CNRS/Université de Savoie-UMR 5041Chemin du Canal – 69 360 SolaizeFranceSearch for other works by this author on:Régis MercierRégis MercierLaboratoire des Matériaux Organiques à Propriétés Spécifiques (LMOPS)CNRS/Université de Savoie-UMR 5041Chemin du Canal – 69 360 SolaizeFranceSearch for other works by this author on:
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Chapter 7: Microwave-assisted Synthesis of Nanomaterials in Aqueous Mediap176-216ByBabita Baruwati;Babita BaruwatiSustainable Technology Division, National Risk Management Research LaboratoryU. S. Environmental Protection Agency26 W. Martin Luther King Dr.MS 443CincinnatiOhio 45268USASearch for other works by this author on:Vivek Polshettiwar;Vivek PolshettiwarSustainable Technology Division, National Risk Management Research LaboratoryU. S. Environmental Protection Agency26 W. Martin Luther King Dr.MS 443CincinnatiOhio 45268USASearch for other works by this author on:
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