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This chapter focuses on the synthesis, design concepts and photovoltaic performance of fullerene-based electron acceptors used in solution processed organic solar cells. Excellent fullerene acceptors such as PCBM, SIMEF, 1,4-di(aryl)fullerenes, diphenylmethanofullerenes, fulleropyrrolidines, ICBA, methano-indene-fullerenes are introduced from a synthetic chemistry viewpoint in addition to fullerene chemistry background being offered, which should benefit a wide range of organic solar cell research.

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