11: Sample Controlled Thermal Analysis
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Published:25 Feb 2016
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Special Collection: RSC eTextbook CollectionProduct Type: Textbooks
G. M. B. Parkes and E. L. Charsley, in Principles of Thermal Analysis and Calorimetry, ed. S. Gaisford, V. Kett, and P. Haines, The Royal Society of Chemistry, 2nd edn, 2016, pp. 232-258.
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Sample controlled thermal analysis (SCTA) methods, where the heating rate is governed by the sample itself, offer a significant number of benefits over conventional thermal analysis methods. The addition of SCTA software to many modern thermal analysis instruments means that it is now readily available. This chapter gives a broad overview of the different approaches to SCTA and their application to a wide range of thermal methods. The benefits of SCTA, which include enhanced resolution and improved kinetic data, are illustrated by applications to a range of materials.