NMR Methods for Characterization of Synthetic and Natural Polymers
Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.
NMR Methods for Characterization of Synthetic and Natural Polymers, The Royal Society of Chemistry, 2019.
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Chapter 1: Applications of NMR in Polymer Characterization – An Introductionp1-22ByKay SaalwächterKay SaalwächterInstitut für Physik – NMR, Martin-Luther-Universität Halle-WittenbergBetty-Heimann-Str. 706120 Halle (Saale)Germany[email protected]Search for other works by this author on:
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Chapter 2: Application of STD NMR in Organic/Inorganic Polymer Materialsp23-35ByYu SuzukiYu SuzukiUniversity of Fukui, Tenure-Track Program for Innovative Research3-9-1, BunkyoFukui-shiFukui910-8507Japan[email protected]Search for other works by this author on:
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Chapter 3: Diffusion and Relaxometry to Study Carbohydrates Dissolved in Ionic Liquidsp36-62ByW. M. Ezzawam;W. M. EzzawamUniversity of Leeds, School of Physics and AstronomyWoodhouse LaneLeedsLS2 9JTUnited Kingdom[email protected]Tripoli University, Department of PhysicsPO Box 13275TripoliLibyaSearch for other works by this author on:M. E. RiesM. E. RiesUniversity of Leeds, School of Physics and AstronomyWoodhouse LaneLeedsLS2 9JTUnited Kingdom[email protected]Search for other works by this author on:
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Chapter 4: High Resolution Magic Angle Spinning (HRMAS) Pulse Field Gradient (PFG) NMR Diffusometry Studies of Swollen Polymersp63-79ByTodd M. AlamTodd M. AlamSandia National Laboratories, Department of Organic Material SciencesMS 0886, PO Box 5800AlbuquerqueNM 87185USA[email protected]Search for other works by this author on:
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Chapter 5: Application of On-line SEC-NMR and DOSY for Practical Polymer Characterizationp80-100ByKoichi Ute;Koichi UteDepartment of Applied Chemistry, Tokushima University2-1 Minami-JosanjimaTokushima 770-8506Japan[email protected]Search for other works by this author on:Ryuhei Nagao;Ryuhei NagaoNitto Analytical Techno-Center Co., Ltd.18 Hirayama NakaharaToyohashi 441-3194JapanSearch for other works by this author on:Kazuya WatanabeKazuya WatanabeResearch and Development Division, Kurita Water Industries Ltd.1-1 Kawada NogiShimotsuga 329-0105JapanSearch for other works by this author on:
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Chapter 6: Dynamics of Polymer Systems Studied by NMR Field-cycling Relaxometryp101-129ByM. Hofmann;M. HofmannExperimentalphysik VII and Nordbayerisches NMR-Zentrum, Universität Bayreuth95440 BayreuthGermany[email protected]Search for other works by this author on:M. Flämig;M. FlämigExperimentalphysik VII and Nordbayerisches NMR-Zentrum, Universität Bayreuth95440 BayreuthGermany[email protected]Search for other works by this author on:E. A. RösslerE. A. RösslerExperimentalphysik VII and Nordbayerisches NMR-Zentrum, Universität Bayreuth95440 BayreuthGermany[email protected]Search for other works by this author on:
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Chapter 7: HR-MAS NMR Characterization of Thermo-responsive Polymer Gels: Network Collapse Dynamics and Intermolecular Interactionsp131-155ByBiaolan Liu;Biaolan LiuState Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, National Center for Magnetic Resonance in Wuhan, Wuhan Institute of Physics and Mathematics, Chinese Academy of SciencesWuhan 430071P. R. China[email protected]Search for other works by this author on:Jiwen FengJiwen FengState Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, National Center for Magnetic Resonance in Wuhan, Wuhan Institute of Physics and Mathematics, Chinese Academy of SciencesWuhan 430071P. R. China[email protected]Search for other works by this author on:
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Chapter 8: Rubber-state NMR Spectroscopyp156-173BySeiichi Kawahara;Seiichi KawaharaNagaoka University of Technology1603-1, Kamitomioka-MachiNagaoka-ShiNiigata940-2188Japan[email protected]Search for other works by this author on:Yoshimasa Yamamoto;Yoshimasa YamamotoDepartment of Mechanical Engineering, National Institute of Technology, Tokyo College1220-2 Kunugida-machiHachioji-shiTokyo 193-0997JapanSearch for other works by this author on:Takayuki SaitoTakayuki SaitoChemicals Evaluation and Research Institute, Japan1600, Shimo-Takano, Sugito-MachiKitakatusika-Gun, Saitama345-0043JapanSearch for other works by this author on:
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Chapter 9: Polymer Blends, Nanocomposites, Rubbers and π-Conjugated Polymersp175-210ByA. AsanoA. AsanoNational Defense Academy, Department of Applied ChemistryHashirimizu 1-10-20Yokosuka239-8686Japan[email protected]Search for other works by this author on:
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Chapter 10: NMR Investigations of Interfaces in Tapered and Inverse-tapered Copolymers in the Solid Statep211-230ByNathan T. Pickering;Nathan T. PickeringOklahoma State University, Department of ChemistryStillwaterOK74078USASearch for other works by this author on:Jeffery L. WhiteJeffery L. WhiteSearch for other works by this author on:
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Chapter 11: Nanostructures, Conformations, and Intermolecular Interactions in Natural Biopolymers Revealed by Solid-state NMR Spectroscopyp231-250ByFenfen Wang;Fenfen WangKey Laboratory of Functional Polymer Materials of Ministry of Education and College of Chemistry, State Key Laboratory of Medicinal Chemical Biology, Nankai UniversityTianjin 300071China[email protected]Search for other works by this author on:Donglin Tian;Donglin TianKey Laboratory of Functional Polymer Materials of Ministry of Education and College of Chemistry, State Key Laboratory of Medicinal Chemical Biology, Nankai UniversityTianjin 300071China[email protected]Search for other works by this author on:Rongchun Zhang;Rongchun ZhangSouth China Advanced Institute for Soft Matter Science and Technology (AISMST), School of Molecular Science and Engineering, South China University of TechnologyGuangzhou510640China[email protected]Search for other works by this author on:Pingchuan SunPingchuan SunKey Laboratory of Functional Polymer Materials of Ministry of Education and College of Chemistry, State Key Laboratory of Medicinal Chemical Biology, Nankai UniversityTianjin 300071China[email protected]Search for other works by this author on:
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Chapter 12: Chain Proximity of Polystyrene in Bulk Polymer, Polymer Blend and Nanocompositesp251-270ByXiaoliang WangXiaoliang WangKey Laboratory of High Performance Polymer Materials and Technology of Ministry of Education, Department of Polymer Science and Engineering, School of Chemistry and Chemical Engineering, State Key Laboratory of Coordination Chemistry, Nanjing UniversityNanjing 210023P. R. China[email protected]Search for other works by this author on:
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Chapter 13: Dipolar Based NMR Methods for Probing Intermediate Regime Motions in Polymersp271-298ByJefferson G. Filgueiras;Jefferson G. FilgueirasInstitute of Physics of São Carlos, University of São Paulo13566-590 São Carlos-SPBrazil[email protected]Search for other works by this author on:Marcio F. Cobo;Marcio F. CoboBruker BioSpin GmbH76287 RheinstettenGermanySearch for other works by this author on:Gregório C. Faria;Gregório C. FariaInstitute of Physics of São Carlos, University of São Paulo13566-590 São Carlos-SPBrazil[email protected]Search for other works by this author on:Tiago B. Moraes;Tiago B. MoraesInstitute of Physics of São Carlos, University of São Paulo13566-590 São Carlos-SPBrazil[email protected]Search for other works by this author on:Eduardo R. de AzevedoEduardo R. de AzevedoInstitute of Physics of São Carlos, University of São Paulo13566-590 São Carlos-SPBrazil[email protected]Search for other works by this author on:
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Chapter 14: Structure and Molecular Dynamics of Semicrystalline Polymers as Studied by Solid-state NMRp299-324ByZhaoxi Zheng;Zhaoxi ZhengThe University of Akron, Department of Polymer Science170 University Ave.AkronOhio 44325-3909USA[email protected]Search for other works by this author on:Jiayang Ma;Jiayang MaThe University of Akron, Department of Polymer Science170 University Ave.AkronOhio 44325-3909USA[email protected]Search for other works by this author on:Kun Wang;Kun WangThe University of Akron, Department of Polymer Science170 University Ave.AkronOhio 44325-3909USA[email protected]Search for other works by this author on:Fan Jin;Fan JinThe University of Akron, Department of Polymer Science170 University Ave.AkronOhio 44325-3909USA[email protected]Search for other works by this author on:Toshikazu MiyoshiToshikazu MiyoshiThe University of Akron, Department of Polymer Science170 University Ave.AkronOhio 44325-3909USA[email protected]Search for other works by this author on:
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Chapter 15: Solid-state NMR of Organic Electronicsp325-362ByRyan NieuwendaalRyan NieuwendaalMaterials Science and Engineering Division, National Institute of Standards and Technology100 Bureau DriveGaithersburgMD 20899-8541USA[email protected]Search for other works by this author on:
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Chapter 16: Molecular Chain Packing and Conformation in π-Conjugated Polymers from Solid-state NMRp363-386ByPhilipp Selter;Philipp SelterWestfälische Wilhelms-Universität Münster, Institute for Physical Chemistry, Correnstr. 28/30, MünsterDE-48149Germany[email protected]Search for other works by this author on:Michael Ryan HansenMichael Ryan HansenWestfälische Wilhelms-Universität Münster, Institute for Physical Chemistry, Correnstr. 28/30, MünsterDE-48149Germany[email protected]Search for other works by this author on:
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Chapter 17: Applications of Solid-state NMR in Crystalline Solid Polymer Electrolytesp387-419ByXiaobin Fu;Xiaobin FuShanghai Key Laboratory of Magnetic Resonance, School of Physics and Materials Science, East China Normal UniversityShanghai200062China[email protected]Department of Molten Salt Chemistry and Engineering, Shanghai Institute of Applied Physics, Chinese Academy of ScienceShanghai201800ChinaSearch for other works by this author on:Qun Chen;Qun ChenShanghai Key Laboratory of Magnetic Resonance, School of Physics and Materials Science, East China Normal UniversityShanghai200062China[email protected]Search for other works by this author on:Ye-Feng YaoYe-Feng YaoShanghai Key Laboratory of Magnetic Resonance, School of Physics and Materials Science, East China Normal UniversityShanghai200062China[email protected]Search for other works by this author on:
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Chapter 18: NMR Characterization of Silkp420-456ByChengchen Guo;Chengchen GuoSchool of Molecular Sciences, Magnetic Resonance Research Center, Arizona State UniversityTempeAZ 85287-1604USASearch for other works by this author on:Jeffery L. YargerJeffery L. YargerSchool of Molecular Sciences, Magnetic Resonance Research Center, Arizona State UniversityTempeAZ 85287-1604USASearch for other works by this author on:
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Chapter 19: Solid-state NMR and Membrane Proteins: Key Interactions in Biomacromoleculesp457-479ByArisu Shigeta;Arisu ShigetaYokohama National University, Graduate School of EngineeringTokiwadai 79-5, Hodogaya-kuYokohama240-8501Japan[email protected]Search for other works by this author on:Izuru KawamuraIzuru KawamuraYokohama National University, Graduate School of EngineeringTokiwadai 79-5, Hodogaya-kuYokohama240-8501Japan[email protected]Search for other works by this author on:
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Chapter 20: Development of Sulfur-33 Nuclear Magnetic Resonance for Structural Study of Crosslinked Rubberp481-505ByKazuhiko YamadaKazuhiko YamadaKochi University, Interdisciplinary Science Unit, Multidisciplinary Sciences Cluster, Research and Education FacultyNankoku CityKochi 783-8505Japan[email protected]Search for other works by this author on:
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Chapter 21: Very Fast MAS NMR >60 kHz for Structural Elucidationp506-532ByYusuke Nishiyama;Yusuke NishiyamaJEOL RESONANCE Inc.AkishimaTokyo 196-8558JapanNMR Science and Development Division, RIKEN SPring-8 CenterYokohamaKanagawa 230-0045JapanSearch for other works by this author on:You-lee HongYou-lee HongInstitute for Integrated Cell-Material Sciences (WPI-iCeMS), Institute for Advanced Study, and AIST-Kyoto University Chemical Energy Materials Open Innovation Laboratory (ChEM-OIL), Kyoto UniversityYoshida, Sakyo-kuKyoto 606-8501JapanSearch for other works by this author on:
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Chapter 22: Structural Investigations of Polymer Materials by Dynamic Nuclear Polarisation Solid-state NMRp533-554ByFabio Ziarelli;Fabio ZiarelliAix Marseille Univ, CNRS, Centrale Marseille, FSCMFR1739F-13397 MarseilleFranceSearch for other works by this author on:Stéphane VielStéphane VielInstitut Universitaire de FranceF-75005ParisFranceSearch for other works by this author on:
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