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Over the past two decades, the unique properties of engineered nanoparticles (NPs) have placed them at the centre of revolutionary advancements in many sectors of science, technology and commerce. Multi-technique and multi-disciplinary analytical approaches are required to identify, quantify, and characterize the chemical composition, size and size distribution, surface properties and the number and concentration of NPs. In this chapter, an overview of the recent advances in the characterization of NPs will be presented.

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