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This chapter reviews methods for the creation and manipulation of singlet order based on spin-locking pulses. Long, weak RF pulses can be used to bring singlet and triplet states into resonance, enabling the creation of singlet order from triplet magnetization, transfer of singlet order between spin pairs, and measurements of spectroscopic parameters in the strong-coupling regime. Applications in NMR spectroscopy and para-hydrogen induced polarization are discussed.

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